Preparation method of platy SAPO (Silicon Aluminum Phosphate)-34 molecular sieve

The invention relates to a preparation method of a platy SAPO (Silicon Aluminum Phosphate)-34 molecular sieve. The preparation method comprises the following steps: mixing a cubical SAPO-34 molecularsieve with a water solution of isopropylamine, then carrying out hydrothermal treatment for 1 to 7 da...

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Hauptverfasser: ZHANG TAO, SONG DIANHUA, WANG JIE, WEN XIAOJIANG, GUO YONG, TAO WANYU, JIANG YU, CUI YUE, ZHANG WENSHAN, ZHANG HAIRONG, LIU YIDING
Format: Patent
Sprache:chi ; eng
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Zusammenfassung:The invention relates to a preparation method of a platy SAPO (Silicon Aluminum Phosphate)-34 molecular sieve. The preparation method comprises the following steps: mixing a cubical SAPO-34 molecularsieve with a water solution of isopropylamine, then carrying out hydrothermal treatment for 1 to 7 days at 140 to 180 DEG C, and washing and drying after cooling, thus obtaining the platy SAPO-34 molecular sieve. By controlling the concentration, the reaction temperature and the time of the isopropylamine, the platy SAPO-34 molecular sieve in controllable thickness can be obtained. According to the preparation method disclosed by the invention, the purpose of preparing platy SAPO-34 molecular sieves in different thicknesses can be achieved by controlling the concentration, the reaction temperature and the time of the isopropylamine on the basis of the cubical SAPO-34 molecular sieve. 本发明涉及种片状SAPO-34分子筛的制备方法,将立方形SAPO-34分子筛与异丙胺的水溶液混合,然后在140~180℃下水热处理1~7天,冷却后洗涤、干燥,即得片状SAPO-34分子筛;通过控制异丙胺浓度、反应温度和时间获得以获得厚度可控的上述片状SAPO-34