Hydrated lead oxychloride micro-nano structured crystal preparation method
The invention belongs to the technical field of micro-nano material preparation and discloses a hydrated lead oxychloride micro-nano structured crystal preparation method. The method includes steps: dissolving lead chloride in deionized water, adding triethylamine under a heating condition, and perf...
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| Format: | Patent |
| Sprache: | chi ; eng |
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| Zusammenfassung: | The invention belongs to the technical field of micro-nano material preparation and discloses a hydrated lead oxychloride micro-nano structured crystal preparation method. The method includes steps: dissolving lead chloride in deionized water, adding triethylamine under a heating condition, and performing reaction to obtain hydrated lead oxychloride micro-nano structured crystal. Hydrated lead oxychloride micro-nano structured crystal powder is obtained by suction filtration and drying. The hydrated lead oxychloride micro-nano structured crystal is flaky, a diameter range is about 80nm-1000nm,and a thickness range is about 40nm-120nm. The method has advantages of simple synthesis process, high repeatability, low cost, safety and environmental friendliness. Therefore, the method is high invalue no matter in laboratory researches or industrial application.
本发明公开了种水合氯氧化铅微纳结构晶体的制备方法，其制备方法属于微纳米材料制备技术领域。本方法用去离子水溶解氯化铅，升温条件下加入三乙胺反应，得到水合氯氧化铅微纳结构晶体。通过抽滤和烘干得到水合氯氧化铅微纳结构晶体的粉末。水合氯氧化铅微纳结构晶体为片状，直径范围约为80 nm-1000 nm，厚度范围约为40 n |
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