Application of Chinese clematis root in separation and preparation of 5-hydroxymethylfurfural

The invention discloses an application of Chinese clematis root in separation and preparation of 5-hydroxymethylfurfural (5-HMF). The application comprises the following steps: extracting Chinese clematis root by using an acidic solution, performing concentration, performing centrifugation, and perf...

Ausführliche Beschreibung

Gespeichert in:
Bibliographische Detailangaben
Hauptverfasser: XU CHENXIN, ZHANG HAIJIANG, LIU WENJIE, JIN FAN, ZANG WANRONG, FU XINXIN, LI YUNJIAN, WEI DANDAN, TANG SEN, ZHAO YUANYUAN, ZHANG QIN, YU JIAMIN
Format: Patent
Sprache:chi ; eng
Schlagworte:
Online-Zugang:Volltext bestellen
Tags: Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
Beschreibung
Zusammenfassung:The invention discloses an application of Chinese clematis root in separation and preparation of 5-hydroxymethylfurfural (5-HMF). The application comprises the following steps: extracting Chinese clematis root by using an acidic solution, performing concentration, performing centrifugation, and performing lyophilization to obtain a crude extract; adding a methanol solution into the crude extract for dissolving, performing centrifugation, taking a supernatant, performing concentration, and adding water for dissolving to obtain a crude extraction liquid containing the 5-hydroxymethylfurfural; performing adsorption on the crude extraction liquid by adopting macroporous resin, performing elution, performing detection by adopting high-performance liquid chromatography, merging eluents, and performing concentration to obtain an enriched substance; and performing preparation by using the enriched substance through semi-preparative high-performance liquid chromatography, collecting a fractioncontaining the 5-hydroxym