Preparation method of low-temperature high-nitrogen-doped sodium ion battery anode material

The invention belongs to the technical field of sodium ion batteries, and in particular relates to a preparation method of a low-temperature nitrogen-doped sodium ion battery anode material. The preparation method at least comprises the following steps: dividing corn straw into corn husk and corncob...

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Hauptverfasser: FANG XINRONG, LI SHIHAI, YU WEIYUAN, ZHANG TAO, XU PAN, ZHU KUNQING, CHANG SONG, WANG NA, LI ZHONGYAN, YANG MAN, YOU KUN, SONG XIAONA, YU FENG, ZHANG XINHE, YANG ZHIXIONG, LIU YONG, YANG CONGQIANG, SONG XIAOBO, WANG ZHENGRUI
Format: Patent
Sprache:chi ; eng
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Zusammenfassung:The invention belongs to the technical field of sodium ion batteries, and in particular relates to a preparation method of a low-temperature nitrogen-doped sodium ion battery anode material. The preparation method at least comprises the following steps: dividing corn straw into corn husk and corncob, grinding the corn husk into powder, and thoroughly drying; dipping into a polytetrafluoroethylene(PTFE) reaction kettle containing a dilute sulfuric acid aqueous solution, washing until neutral, thoroughly drying, and then fully grinding; transferring the product into a high temperature tube furnace, heating up to 1100-1300 DEG C, carrying out heat preservation for 1-6 h, and naturally cooling to the room temperature; soaking the product in a mixed solution of nitric acid and hydrogen peroxide, continuously stirring, then adding distilled water with the same volume, continuously stirring, then washing the obtained sample, and fully drying; transferring the dried sample into an ethylenediamine solution, heating up