Preparation method of low-temperature high-nitrogen-doped sodium ion battery anode material
The invention belongs to the technical field of sodium ion batteries, and in particular relates to a preparation method of a low-temperature nitrogen-doped sodium ion battery anode material. The preparation method at least comprises the following steps: dividing corn straw into corn husk and corncob...
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Format: | Patent |
Sprache: | chi ; eng |
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Zusammenfassung: | The invention belongs to the technical field of sodium ion batteries, and in particular relates to a preparation method of a low-temperature nitrogen-doped sodium ion battery anode material. The preparation method at least comprises the following steps: dividing corn straw into corn husk and corncob, grinding the corn husk into powder, and thoroughly drying; dipping into a polytetrafluoroethylene(PTFE) reaction kettle containing a dilute sulfuric acid aqueous solution, washing until neutral, thoroughly drying, and then fully grinding; transferring the product into a high temperature tube furnace, heating up to 1100-1300 DEG C, carrying out heat preservation for 1-6 h, and naturally cooling to the room temperature; soaking the product in a mixed solution of nitric acid and hydrogen peroxide, continuously stirring, then adding distilled water with the same volume, continuously stirring, then washing the obtained sample, and fully drying; transferring the dried sample into an ethylenediamine solution, heating up |
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