Continuous reaction process for methyltris(methylethylketoxime)silane

Continuous reaction process for methyltris(methylethylketoxime)silane

The invention discloses a continuous reaction process for methyltris(methylethylketoxime)silane. The continuous reaction process comprises the following steps of: continuously metering diacetylmonoxime and cyclohexane in a mass ratio of 1 to (0.5-5) through a mass flow meter, leading diacetylmonoxim...

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Hauptverfasser: YIN SHUBAI, ZENG MANHUA
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Sprache:chi ; eng
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ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAININGELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN,SULFUR, SELENIUM OR TELLURIUM
CHEMISTRY
METALLURGY
ORGANIC CHEMISTRY
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ZENG MANHUA
description The invention discloses a continuous reaction process for methyltris(methylethylketoxime)silane. The continuous reaction process comprises the following steps of: continuously metering diacetylmonoxime and cyclohexane in a mass ratio of 1 to (0.5-5) through a mass flow meter, leading diacetylmonoxime and cyclohexane into a premixing tank, uniformly stirring and mixing in the mixing tank to obtaina material mixture; continuously metering the material mixture in step A through the mass flow meter and feeding the material mixture into a bundled tube reactor; proportioning methyl trichlorosilaneand diacetylmonoxime in a mass ratio of 1 to (0.1-0.3), continuously metering methyl trichlorosilane through the mass flow meter, and feeding the methyl trichlorosilane into the bundled tube reactor through a pump. The continuous reaction process has the advantages of accurate temperature control, safe and reliable performance, small floor space, and simplified management; the bundled tube reactoris adopted, temperature co
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The continuous reaction process comprises the following steps of: continuously metering diacetylmonoxime and cyclohexane in a mass ratio of 1 to (0.5-5) through a mass flow meter, leading diacetylmonoxime and cyclohexane into a premixing tank, uniformly stirring and mixing in the mixing tank to obtaina material mixture; continuously metering the material mixture in step A through the mass flow meter and feeding the material mixture into a bundled tube reactor; proportioning methyl trichlorosilaneand diacetylmonoxime in a mass ratio of 1 to (0.1-0.3), continuously metering methyl trichlorosilane through the mass flow meter, and feeding the methyl trichlorosilane into the bundled tube reactor through a pump. 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subjects ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAININGELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN,SULFUR, SELENIUM OR TELLURIUM
CHEMISTRY
METALLURGY
ORGANIC CHEMISTRY
title Continuous reaction process for methyltris(methylethylketoxime)silane
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