Continuous reaction process for methyltris(methylethylketoxime)silane
The invention discloses a continuous reaction process for methyltris(methylethylketoxime)silane. The continuous reaction process comprises the following steps of: continuously metering diacetylmonoxime and cyclohexane in a mass ratio of 1 to (0.5-5) through a mass flow meter, leading diacetylmonoxim...
Gespeichert in:
Hauptverfasser: | , |
---|---|
Format: | Patent |
Sprache: | chi ; eng |
Schlagworte: | |
Online-Zugang: | Volltext bestellen |
Tags: |
Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
|
Zusammenfassung: | The invention discloses a continuous reaction process for methyltris(methylethylketoxime)silane. The continuous reaction process comprises the following steps of: continuously metering diacetylmonoxime and cyclohexane in a mass ratio of 1 to (0.5-5) through a mass flow meter, leading diacetylmonoxime and cyclohexane into a premixing tank, uniformly stirring and mixing in the mixing tank to obtaina material mixture; continuously metering the material mixture in step A through the mass flow meter and feeding the material mixture into a bundled tube reactor; proportioning methyl trichlorosilaneand diacetylmonoxime in a mass ratio of 1 to (0.1-0.3), continuously metering methyl trichlorosilane through the mass flow meter, and feeding the methyl trichlorosilane into the bundled tube reactor through a pump. The continuous reaction process has the advantages of accurate temperature control, safe and reliable performance, small floor space, and simplified management; the bundled tube reactoris adopted, temperature co |
---|