Continuous reaction process for methyltris(methylethylketoxime)silane

The invention discloses a continuous reaction process for methyltris(methylethylketoxime)silane. The continuous reaction process comprises the following steps of: continuously metering diacetylmonoxime and cyclohexane in a mass ratio of 1 to (0.5-5) through a mass flow meter, leading diacetylmonoxim...

Ausführliche Beschreibung

Gespeichert in:
Bibliographische Detailangaben
Hauptverfasser: YIN SHUBAI, ZENG MANHUA
Format: Patent
Sprache:chi ; eng
Schlagworte:
Online-Zugang:Volltext bestellen
Tags: Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
Beschreibung
Zusammenfassung:The invention discloses a continuous reaction process for methyltris(methylethylketoxime)silane. The continuous reaction process comprises the following steps of: continuously metering diacetylmonoxime and cyclohexane in a mass ratio of 1 to (0.5-5) through a mass flow meter, leading diacetylmonoxime and cyclohexane into a premixing tank, uniformly stirring and mixing in the mixing tank to obtaina material mixture; continuously metering the material mixture in step A through the mass flow meter and feeding the material mixture into a bundled tube reactor; proportioning methyl trichlorosilaneand diacetylmonoxime in a mass ratio of 1 to (0.1-0.3), continuously metering methyl trichlorosilane through the mass flow meter, and feeding the methyl trichlorosilane into the bundled tube reactor through a pump. The continuous reaction process has the advantages of accurate temperature control, safe and reliable performance, small floor space, and simplified management; the bundled tube reactoris adopted, temperature co