Catalytic synthesis method and application of nysted reagent
The invention provides a catalytic synthesis method and application of a nysted reagent. The nysted reagent is an organic solution with a structure shown as a formula (1): the formula (1) is shown inthe description; the catalytic synthesis method of the nysted reagent comprises the following steps:...
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Format: | Patent |
Sprache: | chi ; eng |
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Zusammenfassung: | The invention provides a catalytic synthesis method and application of a nysted reagent. The nysted reagent is an organic solution with a structure shown as a formula (1): the formula (1) is shown inthe description; the catalytic synthesis method of the nysted reagent comprises the following steps: under the protection of inert gas, adding a catalyst copper compound shown as a formula (II) and active zinc powder into an organic solvent; dropwise adding dibromomethane under certain temperature; then raising the temperature and reacting until the zinc powder reacts completely, so as to obtain milky white turbid liquid, namely the nysted reagent. The formula (II) is shown in the description. Compared with the prior art, the catalytic synthesis method and the application of the nysted reagent, provided by the invention, have the greatest advantages that the catalytic synthesis method of the nysted reagent is provided; the formed novel copper compound is used as a catalyst, has a remarkable effect in the synthesis |
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