Hydrothermal crystallization device with alternating temperature field and method for growing crystals by using device

The invention discloses a hydrothermal crystallization device with an alternating temperature field and a method for growing crystals by using the device. The hydrothermal crystallization device comprises a hydrothermal high-pressure kettle; the hydrothermal high-pressure kettle comprises a kettle b...

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Bibliographische Detailangaben
Hauptverfasser: LI DONGPING, QIN SHIJIE, ZHANG CHANGLONG, REN MENGDE, HE XIAOLING, LIN FENG, WU WENYUAN, LU FUHUA, ZHOU HAITAO, ZUO YANBIN, WANG JINLIANG
Format: Patent
Sprache:chi ; eng
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Beschreibung
Zusammenfassung:The invention discloses a hydrothermal crystallization device with an alternating temperature field and a method for growing crystals by using the device. The hydrothermal crystallization device comprises a hydrothermal high-pressure kettle; the hydrothermal high-pressure kettle comprises a kettle body; the inner cavity of the kettle body is divided into three parts which sequentially comprise a first raw material dissolving area, a constant-temperature growing area and a second raw material dissolving area from bottom to top; when the hydrothermal high-pressure kettle is placed into a three-section type resistance furnace for heating, the temperature of each area in the inner cavity of the kettle body is controlled by the three-section type resistance furnace, wherein the temperature of the first raw material dissolving area has a certain temperature difference with the temperature of the second raw material dissolving area, and the temperature of the constant-temperature growing areais between the temperatu