Y/EU-1/SBA-15/ASA/MOF composite material and preparation method thereof
The invention provides a Y/EU-1/SBA-15/ASA/MOF composite material and a preparation method thereof. The method comprises the following steps: synthesizing a guiding agent, and synthesizing a small grain size Y-type molecular sieve by adopting a hydrothermal crystallization method; adding surfactant,...
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Format: | Patent |
Sprache: | chi ; eng |
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Zusammenfassung: | The invention provides a Y/EU-1/SBA-15/ASA/MOF composite material and a preparation method thereof. The method comprises the following steps: synthesizing a guiding agent, and synthesizing a small grain size Y-type molecular sieve by adopting a hydrothermal crystallization method; adding surfactant, EU-1 and SBA-15 molecular sieve slurry and alkaline aluminum-source solution into the slurry containing molecular sieve, and washing, drying and roasting the product to obtain Y/EU-1/SBA-15/ASA complex; uniformly mixing and stirring with a metal salt aqueous solution, and drying to obtain a metal-loaded Y/EU-1/SBA-15/ASA composite material; adding carboxyl-containing organic acid into an organic solvent of alcohol and amide, and uniformly mixing to obtain organic mixture; and adding the metal-loaded Y/EU-1/SBA-15/ASA material into the organic mixture, uniformly stirring, and reacting to obtain the Y/EU-1/SBA-15/ASA/MOF composite material.
本发明提供了种Y/EU-1/SBA-15/ASA/MOF复合材料及其制备方法,包括:先合成导向剂,采用水热晶化法合成小晶粒Y型分子筛,然后在含分子筛的浆 |
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