Magnesium silicon nitride powder and preparation method thereof

The invention relates to magnesium silicon nitride powder and a preparation method thereof. The technical scheme comprises the following steps: using 10-15 wt% of magnesium powder, 15-25 wt% of silica and 65-75 wt% of inorganic salt as raw materials and mixing the raw materials for 0.5-1 h; then und...

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Hauptverfasser: YU CHAO, DENG CHENGJI, CHAI ZHINAN, ZHU HONGXI, DING JUN
Format: Patent
Sprache:chi ; eng
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Zusammenfassung:The invention relates to magnesium silicon nitride powder and a preparation method thereof. The technical scheme comprises the following steps: using 10-15 wt% of magnesium powder, 15-25 wt% of silica and 65-75 wt% of inorganic salt as raw materials and mixing the raw materials for 0.5-1 h; then under the conditions of 0.1-1 MPa and nitrogen atmosphere, heating to a medium temperature at the rate of 5-10 DEG C/min; and heating to firing temperature at the rate of 3-5 DEG C/min, carrying out thermal insulation for 1-7 h, cooling with a furnace, washing, and drying to prepare the magnesium silicon nitride powder. The firing temperature is 900-1300 DEG C, and the temperature difference between the medium temperature and the firing temperature is 100-200 DEG C. The preparation method of the invention has characteristics of simple production process, short production period, rich resources of raw materials and low production cost. The prepared magnesium silicon nitride powder has uniform particle size and single m