2,4,9-trinitro-2,4,9-triaza-7-adamantanol nitrate and synthesis method thereof

The invention discloses a 2,4,9-trinitro-2,4,9-triaza-7-adamantanol nitrate and a synthesis method thereof. According to the synthesis method, triallylcarbinol serving as a raw material is subjected to ozonization, reduction, condensation, dehydrogenation acetylation, nitrolysis and the like to fina...

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Hauptverfasser: LING YIFEI, RUAN HONGWEI, LUO JUN, HOU TIANJIAO, WANG CHENJIAO, SHAO HANGSONG
Format: Patent
Sprache:chi ; eng
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Zusammenfassung:The invention discloses a 2,4,9-trinitro-2,4,9-triaza-7-adamantanol nitrate and a synthesis method thereof. According to the synthesis method, triallylcarbinol serving as a raw material is subjected to ozonization, reduction, condensation, dehydrogenation acetylation, nitrolysis and the like to finally synthesize the 2,4,9-trinitro-2,4,9-triaza-7-adamantanol nitrate. Polynitrohexaazaadamantane and aza-adamantane nitrate prepared by the method have the advantages of symmetrical structures, high density, superior explosion performance, low sensitivity and the like; the 2,4,9-trinitro-2,4,9-triaza-7-adamantanol nitrate can be widely applied to the fields of explosives, propellants, pyrotechnic compounds, fuel and the like. 本发明公开了种2,4,9-三硝基-2,4,9-三氮杂-7-金刚烷醇硝酸酯及其合成方法。以三烯丙基甲醇为原料,经过臭氧化、还原、缩合、脱氢乙酰化、硝解等步骤,最终合成出2,4,9-三硝基-2,4,9-三氮杂-7-金刚烷醇硝酸酯。本发明制得的多硝基氮杂金刚烷及氮杂金刚烷硝酸酯具有结构对称,密度高,爆炸性能优异,感度低等优点,可广泛用于炸药、推进剂、烟火剂和燃料等领域。