Method for producing cured product of episulfide-based resin
The present invention can provide a method for producing a cured product of an episulfide-based resin, the method having: (A) a step for obtaining a composition for a resin by mixing compound (a), compound (b) and a polymerization catalyst; (B) a step for pouring the composition for a resin into a m...
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Zusammenfassung: | The present invention can provide a method for producing a cured product of an episulfide-based resin, the method having: (A) a step for obtaining a composition for a resin by mixing compound (a), compound (b) and a polymerization catalyst; (B) a step for pouring the composition for a resin into a mold; and (C) a step in which, by increasing the temperature of a heating medium, the composition for a resin is polymerized in the heating medium that contains a liquid having a thermal conductivity of 0.2 W/m.K or higher, or in a shower of the heating medium. The maximum temperature of the heating medium in step (C) is 55-110 DEG C. (a) A compound which has two episulfide groups per molecule and which is represented by formula. (1) (b) A compound having one or more thiol groups per molecule.
通过本发明,提供环硫系树脂固化物的制造方法,其依次具有:工序(A):将下述(a)化合物、下述(b)化合物和聚合催化剂混合而得到树脂用组合物;工序(B):向铸模中注入该树脂用组合物;和工序(C):在包含导热率为0.2W/m·K以上液体的热介质中或者在该热介质的淋浴中,使所述热介质的温度升温而使所述树脂用组合物聚合,所述工序(C)中的热介质的最高温度为55~110℃。(a)下述(1)式所表示的分子内具有2个环硫基的化合物;(b)1分子中具有1个以上巯基 |
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