Preparation method of super-hydrophilic polyurethane used as long-acting antifogging agent
The invention provides a preparation method of super-hydrophilic polyurethane used as a long-acting antifogging agent, comprising the following steps: adding acrylic acid grafted modified polyester polyol into a reaction kettle; dehydrating at 100 DEG C to 150 DEG C in vacuum for 1h to 4h; after coo...
Gespeichert in:
Hauptverfasser: | , , , , |
---|---|
Format: | Patent |
Sprache: | chi ; eng |
Schlagworte: | |
Online-Zugang: | Volltext bestellen |
Tags: |
Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
|
Zusammenfassung: | The invention provides a preparation method of super-hydrophilic polyurethane used as a long-acting antifogging agent, comprising the following steps: adding acrylic acid grafted modified polyester polyol into a reaction kettle; dehydrating at 100 DEG C to 150 DEG C in vacuum for 1h to 4h; after cooling to a room temperature, adding hexamethylene diisocyanate and adding acetone for dissolving; raising the temperature to 80 DEG C to 90 DEG C and dropwise adding a catalyst; reacting for 1.5h to 3h to obtain a pre-polymer; adding 2-hydroxy-3-(2-allyloxy)-1-sodium propylsulfonate salt into the pre-polymer and continually reacting for 0.5h; then adding silicon-containing diol and dihydromethyl propionic acid; raising the temperature to 60 DEG C to 75 DEG C and carrying out a chain extension reaction for 1h to 1.5h; after cooling to the room temperature, adding triethylamine under high-speed stirring and stirring for 5min to 10min; adding water for emulsifying to obtain the super-hydrophilic polyurethane. When bein |
---|