Synthesis method and application of quaternary ammonium salt (tetradecyl-dimethyl-benzyl ammonium chloride)

The invention relates to a synthesis method of a quaternary ammonium salt (tetradecyl-dimethyl-benzyl ammonium chloride). The method comprises the following steps: adding dimethylamine and a chlorotetradecane water solution into a quartz test tube, reacting under microwave conditions for 2 minutes,...

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Hauptverfasser: HUANG SHAOSONG, TONG SHANLING, YAN YAN, KE JINCHI, WU YAHONG, YAN HAN
Format: Patent
Sprache:chi ; eng
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Zusammenfassung:The invention relates to a synthesis method of a quaternary ammonium salt (tetradecyl-dimethyl-benzyl ammonium chloride). The method comprises the following steps: adding dimethylamine and a chlorotetradecane water solution into a quartz test tube, reacting under microwave conditions for 2 minutes, and separating through a separating funnel to obtain supernatant grease; and purifying by rotary evaporation under reduced pressure to obtain tetradecyl-dimethyl amine, adding benzyl chloride to prepare the tetradecyl-dimethyl-benzyl ammonium chloride, purifying and drying. The method reduces the organic solvent consumption, is green and environment-friendly, shortens the time and enhances the yield. The tetradecyl-dimethyl-benzyl ammonium chloride can be directly used for preparing a solution which is used for sterilization and alga removal. 季铵盐(十四烷基-二甲基-苄基氯化铵)的合成方法,包括如下步骤:二甲胺和氯代十四烷水溶液加入到石英试管中,微波条件下反应2分钟,分液漏斗分离;得到上层油状物,减压旋转蒸发提纯,得到十四烷基-二甲基胺,加入氯化苄,制备十四烷基-二甲基-苄基氯化铵,纯化干燥,本发明方法减少有机溶剂的使用,绿色环保,时间缩短,产率提高。可以以直接配制溶液,用于杀菌和除藻