Reverse-phase polymerisation process

A reverse-phase suspension polymerisation process for the manufacture of polymer beads comprising forming aqueous monomer beads comprising an aqueous solution of water-soluble ethylenically unsaturated monomer or monomer blend and polymerising the monomer or monomer blend, to form polymer beads whil...

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Hauptverfasser: HESSE PASCAL, NAYLOR GARETH IAN, BARRATT JOHN SCOTT, JELICIC ALEKSANDRA, FONSECA ZEPEDA GABRIELA EUGENIA, LIEVRE MARCEL, KEELAPANDAL RAMAMOORTHY SHANKARA NARAYANAN, SOETJE OLIVER, RAINAU FLORIAN, LEBKUCHER MARK, HASCHICK ROBERT
Format: Patent
Sprache:chi ; eng
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Zusammenfassung:A reverse-phase suspension polymerisation process for the manufacture of polymer beads comprising forming aqueous monomer beads comprising an aqueous solution of water-soluble ethylenically unsaturated monomer or monomer blend and polymerising the monomer or monomer blend, to form polymer beads while suspended in a non-aqueous liquid, and recovering polymer beads, in which the process comprises providing in a vessel (1) a volume (2) of non-aqueous liquid wherein the volume of non-aqueous liquid extends between at least one polymer bead discharge point (3) and at least one monomer feed point (4), feeding the aqueous monomer or monomer blend through orifices (5) into, or onto, the non-aqueous liquid to form aqueous monomer beads, allowing the aqueous monomer beads to flow towards the polymer bead discharge point initiating polymerisation of the aqueous monomer beads to form polymerising beads, wherein the polymerising beads form polymer beads when they reach the polymer bead discharge point, removing a suspensi