Preparation method for magnetic carbon microsphere surface cephalexin molecular imprinted adsorbent material

The present invention relates to a preparation method for a magnetic carbon microsphere surface cephalexin molecular imprinted adsorbent material. The method comprises: taking a walnut shell as a carbon source to prepare a magnetic carbon microsphere; carrying out ethylene functionalized modificatio...

Ausführliche Beschreibung

Gespeichert in:
Bibliographische Detailangaben
Hauptverfasser: LUO SHITIAN, MAO YANLI, CHEN SONGTAO, KANG HAIYAN, WANG ZENGXIN, WU JUNFENG, GUO YIFEI, WANG HONGQIANG
Format: Patent
Sprache:eng
Schlagworte:
Online-Zugang:Volltext bestellen
Tags: Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
Beschreibung
Zusammenfassung:The present invention relates to a preparation method for a magnetic carbon microsphere surface cephalexin molecular imprinted adsorbent material. The method comprises: taking a walnut shell as a carbon source to prepare a magnetic carbon microsphere; carrying out ethylene functionalized modification on the surface of the magnetic carbon microsphere by use of 3-(methacryloxy)propyl trimethoxysilane; taking cephalexin (CFX) as a template molecule, methacrylic acid (MAA) as a functional monomer, ethylene alcohol dimethacrylate (EGDMA) and N, N- methylene bisacrylamide (BIS) as a crosslinking agent, and cetane as a porogenic diluent and an organic solvent to prepare a magnetic carbon microsphere surface imprinted adsorbent. The magnetic carbon microsphere surface imprinted adsorbent material prepared by the method disclosed by the invention is low in cost and simple in preparation, and has high recognition, high selectivity, and high separation enrichment capacity on target molecules, and a high absorption speed.