Ion-absorbed rare earth mother solution treatment recycling method

The invention discloses an ion-absorbed rare earth mother solution treatment recycling method. The method comprises the following steps: firstly carrying out sand filtration, safety filtration, ultrafiltration and nanofiltration on the mother solution to be treated to obtain concentrated water and p...

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Hauptverfasser: SHAO LI'NAN, YANG XIAOSONG, LIU FENGBIAO, LIU YANLI
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creator SHAO LI'NAN
YANG XIAOSONG
LIU FENGBIAO
LIU YANLI
description The invention discloses an ion-absorbed rare earth mother solution treatment recycling method. The method comprises the following steps: firstly carrying out sand filtration, safety filtration, ultrafiltration and nanofiltration on the mother solution to be treated to obtain concentrated water and permeating water, wherein the concentrated water is used as ion-absorbed rare earth concentrated mother solution and the permeating water returns to a liquid mixing tank for mixing liquid; adding 10% sodium sulphide solution into the concentrated water, continuously stirring uniformly with an air pump and carrying out solid-liquid separation by using a centrifuging machine, wherein the separated supernate is concentrated impurity-free liquid and precipitate generated after solid-liquid separation is impurity-free residue; adding saturated ammonium bicarbonate into the concentrated impurity-free liquid, continuously stirring uniformly with the air pump and carrying out precipitate aging crystallization and centrifugal solid-liquid separation. By virtue of the method disclosed by the invention, the problems of an existing impurity removal-precipitate recycling process that facilities cannot be reused and the automation level is low can be solved, the rare earth recovery rate is improved and environment pollution is reduced.
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The method comprises the following steps: firstly carrying out sand filtration, safety filtration, ultrafiltration and nanofiltration on the mother solution to be treated to obtain concentrated water and permeating water, wherein the concentrated water is used as ion-absorbed rare earth concentrated mother solution and the permeating water returns to a liquid mixing tank for mixing liquid; adding 10% sodium sulphide solution into the concentrated water, continuously stirring uniformly with an air pump and carrying out solid-liquid separation by using a centrifuging machine, wherein the separated supernate is concentrated impurity-free liquid and precipitate generated after solid-liquid separation is impurity-free residue; adding saturated ammonium bicarbonate into the concentrated impurity-free liquid, continuously stirring uniformly with the air pump and carrying out precipitate aging crystallization and centrifugal solid-liquid separation. By virtue of the method disclosed by the invention, the problems of an existing impurity removal-precipitate recycling process that facilities cannot be reused and the automation level is low can be solved, the rare earth recovery rate is improved and environment pollution is reduced.</description><language>eng</language><subject>CHEMISTRY ; CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION ORPROCESSING OF GOODS ; COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM,CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THERARE-EARTH METALS ; FERROUS OR NON-FERROUS ALLOYS ; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC ; GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS ; INORGANIC CHEMISTRY ; METALLURGY ; PRETREATMENT OF RAW MATERIALS ; PRODUCTION AND REFINING OF METALS ; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS ; TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINSTCLIMATE CHANGE ; TREATMENT OF ALLOYS OR NON-FERROUS METALS ; TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE</subject><creationdate>2015</creationdate><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&amp;date=20150624&amp;DB=EPODOC&amp;CC=CN&amp;NR=104724854A$$EHTML$$P50$$Gepo$$Hfree_for_read</linktohtml><link.rule.ids>230,308,776,881,25542,76290</link.rule.ids><linktorsrc>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&amp;date=20150624&amp;DB=EPODOC&amp;CC=CN&amp;NR=104724854A$$EView_record_in_European_Patent_Office$$FView_record_in_$$GEuropean_Patent_Office$$Hfree_for_read</linktorsrc></links><search><creatorcontrib>SHAO LI'NAN</creatorcontrib><creatorcontrib>YANG XIAOSONG</creatorcontrib><creatorcontrib>LIU FENGBIAO</creatorcontrib><creatorcontrib>LIU YANLI</creatorcontrib><title>Ion-absorbed rare earth mother solution treatment recycling method</title><description>The invention discloses an ion-absorbed rare earth mother solution treatment recycling method. The method comprises the following steps: firstly carrying out sand filtration, safety filtration, ultrafiltration and nanofiltration on the mother solution to be treated to obtain concentrated water and permeating water, wherein the concentrated water is used as ion-absorbed rare earth concentrated mother solution and the permeating water returns to a liquid mixing tank for mixing liquid; adding 10% sodium sulphide solution into the concentrated water, continuously stirring uniformly with an air pump and carrying out solid-liquid separation by using a centrifuging machine, wherein the separated supernate is concentrated impurity-free liquid and precipitate generated after solid-liquid separation is impurity-free residue; adding saturated ammonium bicarbonate into the concentrated impurity-free liquid, continuously stirring uniformly with the air pump and carrying out precipitate aging crystallization and centrifugal solid-liquid separation. By virtue of the method disclosed by the invention, the problems of an existing impurity removal-precipitate recycling process that facilities cannot be reused and the automation level is low can be solved, the rare earth recovery rate is improved and environment pollution is reduced.</description><subject>CHEMISTRY</subject><subject>CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION ORPROCESSING OF GOODS</subject><subject>COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM,CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THERARE-EARTH METALS</subject><subject>FERROUS OR NON-FERROUS ALLOYS</subject><subject>GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC</subject><subject>GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS</subject><subject>INORGANIC CHEMISTRY</subject><subject>METALLURGY</subject><subject>PRETREATMENT OF RAW MATERIALS</subject><subject>PRODUCTION AND REFINING OF METALS</subject><subject>TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS</subject><subject>TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINSTCLIMATE CHANGE</subject><subject>TREATMENT OF ALLOYS OR NON-FERROUS METALS</subject><subject>TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE</subject><fulltext>true</fulltext><rsrctype>patent</rsrctype><creationdate>2015</creationdate><recordtype>patent</recordtype><sourceid>EVB</sourceid><recordid>eNqNyj0OwjAMBtAuDAi4gzlAJX6CYIUKBAsTe-WmH6RSEleOGbg9CwdgesubVqeb5Jq7ItqhJ2UFgdUCJbEApSLxbYNkMgVbQjZS-I-PQ35RggXp59XkybFg8XNWLS_nR3OtMUqLMrJHhrXNfb1y-4077Nxx-8_5AmrsMoM</recordid><startdate>20150624</startdate><enddate>20150624</enddate><creator>SHAO LI'NAN</creator><creator>YANG XIAOSONG</creator><creator>LIU FENGBIAO</creator><creator>LIU YANLI</creator><scope>EVB</scope></search><sort><creationdate>20150624</creationdate><title>Ion-absorbed rare earth mother solution treatment recycling method</title><author>SHAO LI'NAN ; YANG XIAOSONG ; LIU FENGBIAO ; LIU YANLI</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-epo_espacenet_CN104724854A3</frbrgroupid><rsrctype>patents</rsrctype><prefilter>patents</prefilter><language>eng</language><creationdate>2015</creationdate><topic>CHEMISTRY</topic><topic>CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION ORPROCESSING OF GOODS</topic><topic>COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM,CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THERARE-EARTH METALS</topic><topic>FERROUS OR NON-FERROUS ALLOYS</topic><topic>GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC</topic><topic>GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS</topic><topic>INORGANIC CHEMISTRY</topic><topic>METALLURGY</topic><topic>PRETREATMENT OF RAW MATERIALS</topic><topic>PRODUCTION AND REFINING OF METALS</topic><topic>TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS</topic><topic>TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINSTCLIMATE CHANGE</topic><topic>TREATMENT OF ALLOYS OR NON-FERROUS METALS</topic><topic>TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE</topic><toplevel>online_resources</toplevel><creatorcontrib>SHAO LI'NAN</creatorcontrib><creatorcontrib>YANG XIAOSONG</creatorcontrib><creatorcontrib>LIU FENGBIAO</creatorcontrib><creatorcontrib>LIU YANLI</creatorcontrib><collection>esp@cenet</collection></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext_linktorsrc</fulltext></delivery><addata><au>SHAO LI'NAN</au><au>YANG XIAOSONG</au><au>LIU FENGBIAO</au><au>LIU YANLI</au><format>patent</format><genre>patent</genre><ristype>GEN</ristype><title>Ion-absorbed rare earth mother solution treatment recycling method</title><date>2015-06-24</date><risdate>2015</risdate><abstract>The invention discloses an ion-absorbed rare earth mother solution treatment recycling method. The method comprises the following steps: firstly carrying out sand filtration, safety filtration, ultrafiltration and nanofiltration on the mother solution to be treated to obtain concentrated water and permeating water, wherein the concentrated water is used as ion-absorbed rare earth concentrated mother solution and the permeating water returns to a liquid mixing tank for mixing liquid; adding 10% sodium sulphide solution into the concentrated water, continuously stirring uniformly with an air pump and carrying out solid-liquid separation by using a centrifuging machine, wherein the separated supernate is concentrated impurity-free liquid and precipitate generated after solid-liquid separation is impurity-free residue; adding saturated ammonium bicarbonate into the concentrated impurity-free liquid, continuously stirring uniformly with the air pump and carrying out precipitate aging crystallization and centrifugal solid-liquid separation. By virtue of the method disclosed by the invention, the problems of an existing impurity removal-precipitate recycling process that facilities cannot be reused and the automation level is low can be solved, the rare earth recovery rate is improved and environment pollution is reduced.</abstract><oa>free_for_read</oa></addata></record>
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subjects CHEMISTRY
CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION ORPROCESSING OF GOODS
COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM,CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THERARE-EARTH METALS
FERROUS OR NON-FERROUS ALLOYS
GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC
GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS
INORGANIC CHEMISTRY
METALLURGY
PRETREATMENT OF RAW MATERIALS
PRODUCTION AND REFINING OF METALS
TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINSTCLIMATE CHANGE
TREATMENT OF ALLOYS OR NON-FERROUS METALS
TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
title Ion-absorbed rare earth mother solution treatment recycling method
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