Chemical industrial waste salt refining process

The invention relates to a chemical industrial waste salt refining process which comprises the following steps: pretreating high salt wastewater generated in the production process of aminobenzene ether and p-nitrophenol so as to adjust the pH value, adsorbing by using activated carbon, kieselguhr o...

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Bibliographische Detailangaben
Hauptverfasser: LI LIUDE, MAO YONGSHENG, WU DESHENG, GU JIE
Format: Patent
Sprache:eng
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Beschreibung
Zusammenfassung:The invention relates to a chemical industrial waste salt refining process which comprises the following steps: pretreating high salt wastewater generated in the production process of aminobenzene ether and p-nitrophenol so as to adjust the pH value, adsorbing by using activated carbon, kieselguhr or macroporous resin, removing organisms and organic salts in the wastewater, reducing the COD of the wastewater, neutralizing the high salt wastewater, performing multi-effect evaporation or mechanical recompression so as to evaporate and crystallize, and centrifuging a solid salt; performing high-temperature calcination on the centrifuged solid salt in a rotary kiln or a tunnel kiln, thereby decomposing and oxidizing the organisms at a high temperature, further thoroughly combusting the tail gas generated through calcination in a heat accumulation type tail gas combustion furnace, preheating and recycling the tail gas, performing spraying absorption, dissolving the calcinated salt with water so as to prepare a saturated solution, filtering by using a precise filter, directly supplying the filtrate to ionic membrane caustic soda for use, or performing multi-effect evaporation or mechanical recompression on the filtered saturated salt water so as to evaporate, crystallize and purify, and performing centrifugation, thereby obtaining high-quality solid sodium chloride.