Synthesis method of 5-bromine1-naphthol

The invention discloses a synthesis method of 5-bromine1-naphthol, and belongs to the technical field of organic synthesis. The method comprises the following steps: (1) dissolving 5-bromine-1-naphthylamine into acetic acid, adding sulfuric acid with the mass concentration of 70%-80%, adding a catal...

Ausführliche Beschreibung

Gespeichert in:
Bibliographische Detailangaben
Hauptverfasser: ZHANG YAXUN, GUO QINGZHAO, ZHANG LIPAN, WANG FAYUN, LI DONG, WANG YONG, GUAN BINGFENG, FENG JUNQI, REN ZHAO
Format: Patent
Sprache:eng
Schlagworte:
Online-Zugang:Volltext bestellen
Tags: Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
Beschreibung
Zusammenfassung:The invention discloses a synthesis method of 5-bromine1-naphthol, and belongs to the technical field of organic synthesis. The method comprises the following steps: (1) dissolving 5-bromine-1-naphthylamine into acetic acid, adding sulfuric acid with the mass concentration of 70%-80%, adding a catalyst and reacting at 80-100 DEG C, wherein the catalyst is a metal oxide; and (2) after reaction is ended, cooling, and carrying out suction filtration to obtain a 5-bromine1-naphthol crude product. With the 5-bromine1-naphthol as a raw material, reaction is carried out at ordinary pressure in the presence of the catalyst, so that the method is relatively high in yield, high in maneuverability, relatively low in equipment cost, and wide in industrial popularization prospect.