A method for preparing ethylenediamine by using ethanolamine and ammonia as raw materials

A method for preparing ethylenediamine by using ethanolamine and ammonia as raw materials. Apparatuses adopted in the method comprise a material heater, a reactor for ammonification reactions, a pressure reduction control valve, a gas-liquid separator, a distillation column for removal of the ammoni...

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Hauptverfasser: MA LIXIN, YAN LI, CHEN SHUGUANG, DING YUNJIE, AN LIHUA, DIAO CHENGJI, LV YUAN
Format: Patent
Sprache:chi ; eng
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Zusammenfassung:A method for preparing ethylenediamine by using ethanolamine and ammonia as raw materials. Apparatuses adopted in the method comprise a material heater, a reactor for ammonification reactions, a pressure reduction control valve, a gas-liquid separator, a distillation column for removal of the ammonia, a distillation column for ammonia stripping and a rectification column for ammonia recycling. Raw materials reacts in the presence of hydrogen, the reaction product mixture is subjected to the recovery of ammonia after pressure reduction, and separated aqueous ammonia and liquid ammonia are recycled as a raw material.