Water-proof and oil-repellent magnetic SiO2/Fe3O4 composite particles and preparation method and application thereof
The invention discloses a preparation method of water-proof and oil-repellent magnetic SiO2/Fe3O4 composite particles, which comprises the following steps that: FeCl2 . 4H2O, Na2SO3, polyvinylpyrrolidone, and NaOH are dissolved in deionized water to react for 8h to 16h at a temperature of 100 DEG C...
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Format: | Patent |
Sprache: | chi ; eng |
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Zusammenfassung: | The invention discloses a preparation method of water-proof and oil-repellent magnetic SiO2/Fe3O4 composite particles, which comprises the following steps that: FeCl2 . 4H2O, Na2SO3, polyvinylpyrrolidone, and NaOH are dissolved in deionized water to react for 8h to 16h at a temperature of 100 DEG C to 180 DEG C, and Fe3O4 particles are obtained after separating, washing and drying; and the Fe3O4 particles are uniformly dispersed in ethanol, ammonia is added, TEOS (tetraethyl orthosilicate) is added in stirring, the stirring is continuously carried out for 8h to 16h at a temperature of 5 DEG C to 50 DEG C, and the water-proof and oil-repellent magnetic SiO2/Fe3O4 composite particles are obtained after separating, washing and drying. The performance is improved by preparing a product by wrapping fluorosilane, the production process is simple, the production implementation is strong, and the yield is high. The water-proof and oil-repellent magnetic SiO2/Fe3O4 composite particle or product has better water-proofi |
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