Method for preparing meta-aramid fiber
The invention discloses a method for preparing meta-aramid fiber. The method comprises the following steps of: adding meta-phenylene diamine into a polar solvent; reducing the temperature to be between -10 DEG C and 10 DEG C; gradually adding meta-phthaloyl chloride for reaction; regulating the pH o...
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| creator | SONG XIQUAN LV JIPING PAN SHIDONG SONG CUIYAN |
| description | The invention discloses a method for preparing meta-aramid fiber. The method comprises the following steps of: adding meta-phenylene diamine into a polar solvent; reducing the temperature to be between -10 DEG C and 10 DEG C; gradually adding meta-phthaloyl chloride for reaction; regulating the pH of a reaction solution to be neutral after the reaction; filtering to obtain a spinning solution; heating the spinning solution to the temperature of between 50 DEG C and 120 DEG C; ejecting the spinning solution into a channel through a spinning plate; and removing the solvent in the fiber through a gaseous medium in the channel, and solidifying and molding the fiber to obtain as-spun fiber; soaking the as-spun fiber in a mixed solution of water and organic solvents for certain time; and performing water-washing drawing, drying, molding after heat treatment, cooling and oiling to obtain the meta-aramid fiber. The method for preparing the meta-aramid fiber has the advantages of high spinning speed, and high quality |
| format | Patent |
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The method comprises the following steps of: adding meta-phenylene diamine into a polar solvent; reducing the temperature to be between -10 DEG C and 10 DEG C; gradually adding meta-phthaloyl chloride for reaction; regulating the pH of a reaction solution to be neutral after the reaction; filtering to obtain a spinning solution; heating the spinning solution to the temperature of between 50 DEG C and 120 DEG C; ejecting the spinning solution into a channel through a spinning plate; and removing the solvent in the fiber through a gaseous medium in the channel, and solidifying and molding the fiber to obtain as-spun fiber; soaking the as-spun fiber in a mixed solution of water and organic solvents for certain time; and performing water-washing drawing, drying, molding after heat treatment, cooling and oiling to obtain the meta-aramid fiber. 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The method comprises the following steps of: adding meta-phenylene diamine into a polar solvent; reducing the temperature to be between -10 DEG C and 10 DEG C; gradually adding meta-phthaloyl chloride for reaction; regulating the pH of a reaction solution to be neutral after the reaction; filtering to obtain a spinning solution; heating the spinning solution to the temperature of between 50 DEG C and 120 DEG C; ejecting the spinning solution into a channel through a spinning plate; and removing the solvent in the fiber through a gaseous medium in the channel, and solidifying and molding the fiber to obtain as-spun fiber; soaking the as-spun fiber in a mixed solution of water and organic solvents for certain time; and performing water-washing drawing, drying, molding after heat treatment, cooling and oiling to obtain the meta-aramid fiber. 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The method comprises the following steps of: adding meta-phenylene diamine into a polar solvent; reducing the temperature to be between -10 DEG C and 10 DEG C; gradually adding meta-phthaloyl chloride for reaction; regulating the pH of a reaction solution to be neutral after the reaction; filtering to obtain a spinning solution; heating the spinning solution to the temperature of between 50 DEG C and 120 DEG C; ejecting the spinning solution into a channel through a spinning plate; and removing the solvent in the fiber through a gaseous medium in the channel, and solidifying and molding the fiber to obtain as-spun fiber; soaking the as-spun fiber in a mixed solution of water and organic solvents for certain time; and performing water-washing drawing, drying, molding after heat treatment, cooling and oiling to obtain the meta-aramid fiber. The method for preparing the meta-aramid fiber has the advantages of high spinning speed, and high quality</abstract><oa>free_for_read</oa></addata></record> |
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| subjects | APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBONFILAMENTS CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS,THREADS, FIBRES, BRISTLES OR RIBBONS CHEMISTRY COMPOSITIONS BASED THEREON MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONSONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS MECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OFARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES ORRIBBONS METALLURGY NATURAL OR ARTIFICIAL THREADS OR FIBRES ORGANIC MACROMOLECULAR COMPOUNDS SPINNING TEXTILES THEIR PREPARATION OR CHEMICAL WORKING-UP |
| title | Method for preparing meta-aramid fiber |
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