Process for producing cellulose ether by directly separating and recovering diluent

The invention discloses a process for producing cellulose ether by directly separating and recovering diluent, which comprises the following steps: adding sodium hydroxide and refined cottons into a mixed diluent system to carry out alkalization reaction; then adding etherifying agent into the obtai...

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Bibliographische Detailangaben
Hauptverfasser: QIU JIANJUN, BI XINDE, BI YANHENG, WANG RONGXIN, BI YUDONG, BI YINGDE
Format: Patent
Sprache:chi ; eng
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Beschreibung
Zusammenfassung:The invention discloses a process for producing cellulose ether by directly separating and recovering diluent, which comprises the following steps: adding sodium hydroxide and refined cottons into a mixed diluent system to carry out alkalization reaction; then adding etherifying agent into the obtained mixture to carry out etherification reaction, after the etherification reaction is completed, obtaining a mixed slurry of cellulose ether and organic diluent; and then recycling the organic diluent, and washing and refining the separated cellulose ether so as to obtain a finished product. The process is characterized in that the mixed slurry obtained in the step of etherification reaction is pumped to a centrifugal machine to carry out solid-liquid separation directly; then the obtained liquid mainly comprising the diluent enters into a settling tank to carry out gravity settling, and the obtained liquid subjected to gravity settling is directly used as diluent for recycling; and the obtained solid enters into