Growth method of bismuth silicate monocrystal with hydrothermal method

The invention relates to a growth method of bismuth silicate (Bi12 SiO20, BSO for short) monocrystal with a hydrothermal method. The method is characterized in that crystal growth is executed by taking a fluoride mineralizer system. The method comprises the following steps: taking BSO raw materials...

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Bibliographische Detailangaben
Hauptverfasser: ZHANG CHANGLONG, QIN SHIJIE, HUO HANDE, HE XIAOLING, WANG JINLIANG, ZHOU HAITAO, ZHANG HAIXIA
Format: Patent
Sprache:chi ; eng
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Beschreibung
Zusammenfassung:The invention relates to a growth method of bismuth silicate (Bi12 SiO20, BSO for short) monocrystal with a hydrothermal method. The method is characterized in that crystal growth is executed by taking a fluoride mineralizer system. The method comprises the following steps: taking BSO raw materials as cultivation materials; putting the cultivation materials at the bottom of a golden lining sleeve; putting a golden baffle plate with 7-10% of aperture ratio at the middle lower part of the golden lining sleeve; separating a cultivation materials dissolving region at a lower part from a crystal growing region at an upper part; hanging seed crystal or gold wire at the top of the golden lining sleeve; adding fluoride solution with 0.3-6 mol/L of fluorine ion concentration into the golden lining sleeve according to 65-75% of filling degree; sealing the golden lining sleeve; putting the golden lining sleeve into a high pressure kettle; adding a certain quantity of deionized water or distilled water into an interlayer