Microcoulomb analysis method for chlorinity high-temperature burning of organic phosphate fire-resistant oil and device thereof

The invention belongs to a microcoulomb analysis method for the chlorinity high-temperature burning of organic phosphate fire-resistant oil and a device thereof, belonging to the field of power analysis chemistry and solving the defects of complicated operation steps, long time consumption, unobvious titration end point, poor accuracy and repetitiveness and high cost existing in the prior art. Thedevice comprises a high-temperature furnace and a burning tube inserted in the high-temperature furnace; the burning tube is provided with an oxygen interface, a nitrogen interface and a sample inletand comprises a gasifying section and a burning section, one end of the burning tube is connected with a sample inlet device, and the other end is connected with an electrolytic bath. The device adopts heating, gasifying and electrolytic analysis methods to obtain the chlorinity of a sample. The invention has simple and convenient operation and rapid analysis speed and adopts a microcoulomb method to analyze titration and