Method for preparing ethylene glycol

The invention relates to a method for producing glycol, which mainly solves the problem that catalysts in the prior art are poor in stability and short in regeneration period. By adopting a technical proposal of taking oxalate as raw material, taking polar or nonpolar solvent as thinner and allowing...

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Bibliographische Detailangaben
Hauptverfasser:	ZHU ZHIYAN, LIU JUNTAO, KUAI JUN, WANG WANMIN
Format:	Patent
Sprache:	chi ; eng
Schlagworte:	ACYCLIC OR CARBOCYCLIC COMPOUNDS CHEMISTRY CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION ORPROCESSING OF GOODS GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS METALLURGY ORGANIC CHEMISTRY TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINSTCLIMATE CHANGE
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Beschreibung
Zusammenfassung:	The invention relates to a method for producing glycol, which mainly solves the problem that catalysts in the prior art are poor in stability and short in regeneration period. By adopting a technical proposal of taking oxalate as raw material, taking polar or nonpolar solvent as thinner and allowing the raw material to be in contact with and react with a copper-bearing catalyst so as to form glycol-containing effluent at a temperature between 120 and 300 DEG C, at a weight space velocity between 0.01 and 10 hours, with the hydrogen/ester molar ratio of 5-300:1, under the reaction pressure between 0.1 and 10.0 MPa, under the condition that the mass fraction of the oxalate is between 0.1 and 100 percent, the method solves the problem well, and can be used in the industrial production of glycol.