Preparation of modified active carbon glass chromatography column

The present invention discloses a method for preparing a modified activated charcoal glass chromatography column. The method comprises the following process steps that: a woody material is dried, thermally decomposed and carbonized at a high temperature; charcoal blocks after carbonization are crush...

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Bibliographische Detailangaben
Hauptverfasser: ZHAI LIFEI, XU HENGZHEN, ZHOU CHUANGUANG, YAO ZIWEI
Format: Patent
Sprache:chi ; eng
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Beschreibung
Zusammenfassung:The present invention discloses a method for preparing a modified activated charcoal glass chromatography column. The method comprises the following process steps that: a woody material is dried, thermally decomposed and carbonized at a high temperature; charcoal blocks after carbonization are crushed, ground and sieved so as to obtain charcoal powder; the charcoal powder which is ground and sieved is adequately soaked in a hydrochloric acid solution and a sodium hydroxide solution in turn; the charcoal powder which is soaked in the hydrochloric acid solution and the sodium hydroxide solution and dried is activated in a high-temperature furnace; and the activated charcoal powder after high-temperature activation and anhydrous sodium sulfate are put into a glass chromatography column containing acetone in turn so as to prepare an activated charcoal glass chromatography column. The method for preparing the modified activated charcoal has the advantages of low cost, easy operation and applicability to the separa