Preparation of electronic grade gallic acid by complexation-resin adsorption combined process
The invention discloses a technology to make electronic grade gallic acid that includes the following steps: mixing industrial grade gallic acid with EDTA disodium salt according to 100:0.5-100:2, adding deionized water, heating to fully be dissolved, cooling and crystallizing, filtering, washing by...
Gespeichert in:
1. Verfasser: | |
---|---|
Format: | Patent |
Sprache: | eng |
Schlagworte: | |
Online-Zugang: | Volltext bestellen |
Tags: |
Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
|
Zusammenfassung: | The invention discloses a technology to make electronic grade gallic acid that includes the following steps: mixing industrial grade gallic acid with EDTA disodium salt according to 100:0.5-100:2, adding deionized water, heating to fully be dissolved, cooling and crystallizing, filtering, washing by deionized water to gain gallic acid crystal; adding ion exchanging resin into chromatography, and aspect ratio is 2-10; heating and dissolving crystal gained in the first step by deionized water, passing through chromatography column at 0.5-3.0BV/h, gathering effluent liquid; gaining electronic grade gallic acid after crystallization and drying. The invention has the advantages of high yield, simple technology, and could be used to take electronic component cleaning. |
---|