Verfahren zur kontinuierlichen Herstellung von quaternären Ammoniumverbindungen

Verfahren zur kontinuierlichen Herstellung von quaternären Ammoniumverbindungen

1,260,643. Quaternary ammonium chloride. FARBWERKE HOECHST A.G. 24 Feb., 1970 [25 Feb., 1969], No. 8795/70. Heading C2C. A process for the preparation of a quaternary ammonium chloride having the general formula: wherein R1 is a C 8 -C 22 aliphatic group, R2 is a C 1 -C 22 aliphatic group, and a is...

Ausführliche Beschreibung

Gespeichert in:
Bibliographische Detailangaben
Hauptverfasser: MUELLER-SCHIEDMAYER,GUENTHER,DR, HUEBNER,HERBERT,DR, MUELLER,HEINZ,DR, ULM,KLAUS,DR
Format: Patent
Sprache:ger
Schlagworte:
ACYCLIC OR CARBOCYCLIC COMPOUNDS
CHEMISTRY
METALLURGY
ORGANIC CHEMISTRY
Online-Zugang:Volltext bestellen
Tags: Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
Beschreibung
Zusammenfassung:1,260,643. Quaternary ammonium chloride. FARBWERKE HOECHST A.G. 24 Feb., 1970 [25 Feb., 1969], No. 8795/70. Heading C2C. A process for the preparation of a quaternary ammonium chloride having the general formula: wherein R1 is a C 8 -C 22 aliphatic group, R2 is a C 1 -C 22 aliphatic group, and a is 0 or 1, comprises continuously reacting an amine of the formula with methyl chloride and (2-a) moles of an alkali metal hydroxide per mol of amine at a temperature of from 50 to 90‹ C. in a reaction medium comprising the final product and a low boiling alcohol whilst maintaining a methyl chloride partial pressure of from 3 to 10 atmospheres gauge. The amines used in the examples are distearylamine, di(tallow fatty acid) amine, di- (coconut oil) amine, primary soybean oil amine and a #-branched pentadecylamine.