PRODUCTION OF 1,1,1,2,3,3,3-HEPTAFLUOROPROPANE

Preparation of HFC 227ea by reacting HFP with hydrogen fluoride comprising t he steps of charging the reaction mixture therefrom to a liquid-phase separator , allowing a HFC 227ea-rich phase and a hydrogen fluoride-rich phase to separa te under gravity, recycling the separated hydrogen fluoride-rich...

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Hauptverfasser: GIBSON, ROBIN RIYADH, SUMMERS, GREG LYNDON
Format: Patent
Sprache:eng ; fre
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Zusammenfassung:Preparation of HFC 227ea by reacting HFP with hydrogen fluoride comprising t he steps of charging the reaction mixture therefrom to a liquid-phase separator , allowing a HFC 227ea-rich phase and a hydrogen fluoride-rich phase to separa te under gravity, recycling the separated hydrogen fluoride-rich phase, chargin g the HFC 227ea-rich phase to a distillation column, recovering the HFC 227ea and an HF-rich mixture separately from the distillation column; and recyclin g the HF-rich mixture to the reactor.