DINITRATION OF NITROBENZOTRIFLUORIDE

DINITRATION OF NITROBENZOTRIFLUORIDE This invention relates to an improvement in a process for dinitrating 3-nitrobenzotrifluoride and 4-halo-3-nitro-benzotrifluoride compounds wherein the mononitrobenzotrifluoride composition is contacted with a mixture comprising sulfuric and nitric acid. The impr...

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1. Verfasser: MILLIGAN, BARTON
Format: Patent
Sprache:eng ; fre
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Zusammenfassung:DINITRATION OF NITROBENZOTRIFLUORIDE This invention relates to an improvement in a process for dinitrating 3-nitrobenzotrifluoride and 4-halo-3-nitro-benzotrifluoride compounds wherein the mononitrobenzotrifluoride composition is contacted with a mixture comprising sulfuric and nitric acid. The improvement constituting the basis of this invention comprises carrying out the dinitration with the sulfuric acid being present in at least a catalytic proportion but not exceeding about 65 mole percent in said mixture.