PROCESSO PARA PRODUZIR UM COMPOSTO DE TIOLCARBAMATO

A process for producing a thiolcarbamate compound of the following formula (IV) wherein R1 represents a hydrogen atom, an alkyl group having 1 to 5 carbon atoms, an alkoxy group having 1 to 5 carbon atoms, a halogen atom or a nitro group, R2 represents a hydrogen atom or an alkyl group having 1 to 4...

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Hauptverfasser: KUNIO UCHIMURA, KAZUHIKO KONNO, ATSUSHI GOH
Format: Patent
Sprache:por
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Zusammenfassung:A process for producing a thiolcarbamate compound of the following formula (IV) wherein R1 represents a hydrogen atom, an alkyl group having 1 to 5 carbon atoms, an alkoxy group having 1 to 5 carbon atoms, a halogen atom or a nitro group, R2 represents a hydrogen atom or an alkyl group having 1 to 4 carbon atoms, m is 1 or 2, and n is an integer of 4 to 6, which comprises reacting an alpha -methylstyrene of the following formula (I) wherein R1 is as defined above, or its dimer with hydrogen sulfide in the presence of a catalyst to form a mercaptan of the following formula (II) wherein R1 is as defined above, and reacting the mercaptan of formula (II) with a carbamoyl chloride of the following formula (III) wherein R2, m and n are as defined.