PRODUCTION OF AMMONIUM VANADATE

PRODUCTION OF AMMONIUM VANADATE

of low alkali content is prepd. by precipitating solns. of sodium vanadate and sulphate with ammonium sulphate at pH 7.5 to 9 and at 25-35 degrees C, pref. with vigorous stirring. Higher purity of prod. reduces losses in aluminothermic redn. of V2O5 to vanadium, caused by Na2O, which consumes more A...

Ausführliche Beschreibung

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Bibliographische Detailangaben
Hauptverfasser: HUBERT BINGS, ROLANDE THOME
Format: Patent
Sprache:eng
Schlagworte:
CHEMISTRY
COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSESC01D OR C01F
INORGANIC CHEMISTRY
METALLURGY
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Beschreibung
Zusammenfassung:of low alkali content is prepd. by precipitating solns. of sodium vanadate and sulphate with ammonium sulphate at pH 7.5 to 9 and at 25-35 degrees C, pref. with vigorous stirring. Higher purity of prod. reduces losses in aluminothermic redn. of V2O5 to vanadium, caused by Na2O, which consumes more Al and is reduced to sodium, which causes the dust produced in the process to contain appreciable amts. of vanadium. Yield in the pptn. is raised from 83% to 97%.