Method for detecting elements in solutions and device for realising the same

The present invention pertains to the construction of analytical instruments and may be used for analysing naturel or industrial waters, biological samples as well as geological samples. The method for detecting elements in solutions comprises pulverising the samples using pulses, ionising the pulve...

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Bibliographische Detailangaben
Hauptverfasser: ALEXANDR AKHATOVICH GANEEV, SERGEI EVGENIEVICH SHOLUPOV
Format: Patent
Sprache:eng
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Beschreibung
Zusammenfassung:The present invention pertains to the construction of analytical instruments and may be used for analysing naturel or industrial waters, biological samples as well as geological samples. The method for detecting elements in solutions comprises pulverising the samples using pulses, ionising the pulverised atoms during Penning's collisions and recording the ions thus formed during a mass spectral analysis while carrying out a separation of the ion time- of- flight. The pulse pulverisation of the sample is carried out from a surface which is heated at a temperature of between 1000 and 1500%C and on which the sample dried in a flow of ballast gas forms a dry residue. The ballast gas may consist of Kr, Xe or mixtures thereof wich Ar under a pressure of between 1 and 2 torrs. The device for detecting elements in solutions comprises an ionising device which is arranged in a gas-discharge chamber filled with an inert gas. The detection device further includes a time- of- flight mass spectrometer which comprises an ion sampling and focusing system as well as a reflective mass in the shape of a spectral analyser. The ionising device is made in the shape of a thin-wall, metallic, cylindrical and hollow cathode that comprises a dosing opening which is used for introducing the sample to be analysed and which is located on a same axis with a vacuum port.