METHOD FOR SEQUENTIAL ONE-POT SYNTHESIS OF TKX-50

METHOD FOR SEQUENTIAL ONE-POT SYNTHESIS OF TKX-50

The present invention relates to a sequential one-pot synthesis of TKX-50, suitable for larger-scale production, during which an acetyl halide is used during the cyclization of diazidoglyoxime so as to obtain 1,1'-diacetyl-5,5'-bistetrazole, which is then hydrolysed to 5,5'-bistetrazo...

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Bibliographische Detailangaben
Hauptverfasser: ECK, Geneviève, LACEMON, Frédérick, ALAIME, Thibaud, DELAGE, Arthur, KLAPÖTKE, Thomas, STIERSTORFER, Jörg, BÖLTER, Marc
Format: Patent
Sprache:eng
Schlagworte:
APPARATUS THEREFOR
CHEMISTRY
GENERAL METHODS OF ORGANIC CHEMISTRY
HETEROCYCLIC COMPOUNDS
METALLURGY
ORGANIC CHEMISTRY
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Beschreibung
Zusammenfassung:The present invention relates to a sequential one-pot synthesis of TKX-50, suitable for larger-scale production, during which an acetyl halide is used during the cyclization of diazidoglyoxime so as to obtain 1,1'-diacetyl-5,5'-bistetrazole, which is then hydrolysed to 5,5'-bistetrazole-1,1'-diolate, to which compound a hydroxylammonium salt is subsequently added.