VERFAHREN ZUR HERSTELLUNG VON 14BETA- HYDROXYSTEROIDEN

VERFAHREN ZUR HERSTELLUNG VON 14BETA- HYDROXYSTEROIDEN

A process for the preparation of 14 beta -hydroxysteroids of the general formula I in which R1 is a hydrogen atom or a methyl group and A is the remainder of the steroid molecule, is described and comprises reacting a steroid of the general formula II in which R1 and A have the abovementioned meanin...

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Hauptverfasser: KIRSCH, GERALD, GOLDE, ROLAND, NEEF, GUENTER
Format: Patent
Sprache:ger
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CHEMISTRY
METALLURGY
ORGANIC CHEMISTRY
STEROIDS
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creator KIRSCH, GERALD
GOLDE, ROLAND
NEEF, GUENTER
description A process for the preparation of 14 beta -hydroxysteroids of the general formula I in which R1 is a hydrogen atom or a methyl group and A is the remainder of the steroid molecule, is described and comprises reacting a steroid of the general formula II in which R1 and A have the abovementioned meaning, and R2 is a 1-oxoalkyl radical with 2 to 6 carbon atoms or a benzoyl group, with a nitroso compound of the formula III heating the resulting product in the presence of an alcohol containing 1 to 4 carbon atoms, and partially hydrogenating the compound of the general formula IV prepared in this way in which R1 and A have the abovementioned meaning.f
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subjects CHEMISTRY
METALLURGY
ORGANIC CHEMISTRY
STEROIDS
title VERFAHREN ZUR HERSTELLUNG VON 14BETA- HYDROXYSTEROIDEN
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