Synthesis of high value-added zeolitic materials using glass powder residue as a silica source

In this work, zeolite A was obtained using alkaline fusion followed by a hydrothermal treatment of glass powder residue derived from the manufacturing of glass. The following parameters were evaluated: leaching of the stock material (silica source), mineralizing agent, alumina source, and the alkali...

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Veröffentlicht in:Materials research (São Carlos, São Paulo, Brazil) São Paulo, Brazil), 2014-02, Vol.17 (1), p.213-218
Hauptverfasser: Alves, J. A. B. L. R., Dantas, E. R. S., Pergher, S. B. C., Melo, D. M. A., Melo, M. A. F.
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Sprache:eng
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Zusammenfassung:In this work, zeolite A was obtained using alkaline fusion followed by a hydrothermal treatment of glass powder residue derived from the manufacturing of glass. The following parameters were evaluated: leaching of the stock material (silica source), mineralizing agent, alumina source, and the alkaline fusion and crystallization temperatures. The synthesized materials were characterized by chemical analysis using energy dispersive X-ray analysis (EDX), X-ray diffraction (XRD) and scanning electron microscopy (SEM). The XRD and SEM results showed that zeolite A was obtained under almost all of the evaluated parameters. The use of pseudoboehmite as an aluminum source led to the formation of zeolite X as a secondary phase and a change in the temperature of fusion, which at 500 [degrees]C, there was formation of zeolite A, hydrated sodalite and zeolite X.
ISSN:1516-1439
1980-5373
1980-5373
DOI:10.1590/S1516-14392013005000191