Synthesis of high value-added zeolitic materials using glass powder residue as a silica source
In this work, zeolite A was obtained using alkaline fusion followed by a hydrothermal treatment of glass powder residue derived from the manufacturing of glass. The following parameters were evaluated: leaching of the stock material (silica source), mineralizing agent, alumina source, and the alkali...
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Veröffentlicht in: | Materials research (São Carlos, São Paulo, Brazil) São Paulo, Brazil), 2014-02, Vol.17 (1), p.213-218 |
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Format: | Artikel |
Sprache: | eng |
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Zusammenfassung: | In this work, zeolite A was obtained using alkaline fusion followed by a hydrothermal treatment of glass powder residue derived from the manufacturing of glass. The following parameters were evaluated: leaching of the stock material (silica source), mineralizing agent, alumina source, and the alkaline fusion and crystallization temperatures. The synthesized materials were characterized by chemical analysis using energy dispersive X-ray analysis (EDX), X-ray diffraction (XRD) and scanning electron microscopy (SEM). The XRD and SEM results showed that zeolite A was obtained under almost all of the evaluated parameters. The use of pseudoboehmite as an aluminum source led to the formation of zeolite X as a secondary phase and a change in the temperature of fusion, which at 500 [degrees]C, there was formation of zeolite A, hydrated sodalite and zeolite X. |
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ISSN: | 1516-1439 1980-5373 1980-5373 |
DOI: | 10.1590/S1516-14392013005000191 |