Determination of multiple mycotoxins in maize using quechers sample preparation and LC-MS/MS detection

Determination of multiple mycotoxins in maize using quechers sample preparation and LC-MS/MS detection

A reliable and easy method has been used for the multiple mycotoxins determination of AFs, DON, ZEA and FBs in maize samples. Liquid chromatography cou?pled mass spectrometry (LC-MS/MS) was used. Mycotoxins have been extracted from maize using a QuEChERS-based extraction procedure. All validation pa...

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Veröffentlicht in:Zbornik Matice Srpske za Prirodne Nauke 2017, Vol.2017 (133), p.123-130
Hauptverfasser: Vukovic, Gorica, Kos, Jovana, Bursic, Vojislava, Colovic, Radmilo, Vukmirovic, Djuro, Jajic, Igor, Krstovic, Sasa
Format: Artikel
Sprache:eng
Schlagworte:
AFѕ
DON
FBs
LC-MS/MS
maize
QuEChERS
ZEA
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Zusammenfassung:A reliable and easy method has been used for the multiple mycotoxins determination of AFs, DON, ZEA and FBs in maize samples. Liquid chromatography cou?pled mass spectrometry (LC-MS/MS) was used. Mycotoxins have been extracted from maize using a QuEChERS-based extraction procedure. All validation parameters were in accordance with Reg. (EC) No 401/2006. The analyses of eight maize seed samples showed the AFs, DON, ZEA and FBs contamination with the values below the state limit standards. nema
ISSN:0352-4906
2406-0828
DOI:10.2298/ZMSPN1733123V