Ethyl 12-Sulfamoyl-abieta-8,11,13-trien-18-oate

We synthesized the novel compound ethyl 12-sulfamoyl-abieta-8,11,13-trien-18-oate in good yield from ethyl 12-sulfo-abieta-8,11,13-trien-18-oate via a two-step protocol. The product was comprehensively characterized by one- and two-dimensional NMR methods, single-crystal X-ray diffraction, IR spectr...

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Veröffentlicht in:	MolBank 2023-02, Vol.2023 (1), p.M1584
Hauptverfasser:	Izmest’ev, Evgeniy S, Pestova, Svetlana V, Gerasimova, Darya P, Babaeva, Olga B, Lodochnikova, Olga A, Nikitina, Liliya E, Kayumov, Airat R, Rubtsova, Svetlana A
Format:	Artikel
Sprache:	eng
Schlagworte:	Analysis Chemical synthesis dehydroabietane derivatives Diffraction diterpenoids Fourier transforms Hydrogen bonds Identification and classification Infrared spectroscopy Mass spectrometry Methods NMR Nuclear magnetic resonance Nuclear magnetic resonance spectroscopy single crystal X-ray diffraction Single crystals Software Structure Sulfonamides X-rays
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Beschreibung
Zusammenfassung:	We synthesized the novel compound ethyl 12-sulfamoyl-abieta-8,11,13-trien-18-oate in good yield from ethyl 12-sulfo-abieta-8,11,13-trien-18-oate via a two-step protocol. The product was comprehensively characterized by one- and two-dimensional NMR methods, single-crystal X-ray diffraction, IR spectroscopy, and high-resolution mass spectrometry.
ISSN:	1422-8599 1422-8599
DOI:	10.3390/M1584