Data acquisition of triple quadrupole LC-MS for the citrinin determination

Data acquisition of triple quadrupole LC-MS for the citrinin determination

The analysis of citrinin is challenging because it needs to be detected in low concentrations in complex sample matrices. Before citrinin quantification, the data acquisition of LC-MS/MS must be performed, which includes the determination of ion monitoring reaction (SRM), finding fragmentation energ...

Ausführliche Beschreibung

Gespeichert in:
Bibliographische Detailangaben
Veröffentlicht in:Zbornik Matice Srpske za Prirodne Nauke 2017, Vol.2017 (133), p.131-141
Hauptverfasser: Vukovic, Gorica, Bursic, Vojislava, Aleksic, Goran, Kuzmanovic, Slobodan, Cara, Magdalena, Abd, El-Wahab
Format: Artikel
Sprache:eng
Schlagworte:
CIN
data acquisition
LC-MS/MS
Online-Zugang:Volltext
Tags: Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
Beschreibung
Zusammenfassung:The analysis of citrinin is challenging because it needs to be detected in low concentrations in complex sample matrices. Before citrinin quantification, the data acquisition of LC-MS/MS must be performed, which includes the determination of ion monitoring reaction (SRM), finding fragmentation energies (Frag.) and collision cell energies (CE) for which the response of citrinin will be the highest for the given conditions. The best response of citrinin is obtained for Frag. of 66 V and CE of 17 and 29 V.
ISSN:0352-4906
2406-0828
DOI:10.2298/ZMSPN1733131V