Heitt Mjölnir: a heated miniature triaxial apparatus for 4D synchrotron microtomography

Third‐ and fourth‐generation synchrotron light sources with high fluxes and beam energies enable the use of innovative X‐ray translucent experimental apparatus. These experimental devices access geologically relevant conditions whilst enabling in situ characterization using the spatial and temporal...

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Veröffentlicht in:Journal of synchrotron radiation 2024-01, Vol.31 (1), p.150-161
Hauptverfasser: Freitas, Damien, Butler, Ian B., Elphick, Stephen C., Gilgannon, James, Rizzo, Roberto E., Plümper, Oliver, Wheeler, John, Schlepütz, Christian M., Marone, Federica, Fusseis, Florian
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Sprache:eng
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Zusammenfassung:Third‐ and fourth‐generation synchrotron light sources with high fluxes and beam energies enable the use of innovative X‐ray translucent experimental apparatus. These experimental devices access geologically relevant conditions whilst enabling in situ characterization using the spatial and temporal resolutions accessible at imaging beamlines. Here, Heitt Mjölnir is introduced, a heated miniature triaxial rig based on the design of Mjölnir, but covering a wider temperature range and larger sample volume at similar pressure capacities. This device is designed to investigate coupled thermal, chemical, hydraulic and mechanical processes from grain to centimetre scales using cylindrical samples of 10 mm × 20 mm (diameter × length). Heitt Mjölnir can simultaneously reach confining (hydraulic) pressures of 30 MPa and 500 MPa of axial stress with independently controlled sample pore fluid pressure < 30 MPa. This internally heated apparatus operates to temperatures up to 573 K with a minimal vertical thermal gradient in the sample of
ISSN:1600-5775
0909-0495
1600-5775
DOI:10.1107/S1600577523009876