2-[(2-Carboxyphenyl)disulfanyl]benzoic acid #8211;4,4 #8242;-bipyridyl N,N #8242;-dioxide (1/2)

2-[(2-Carboxyphenyl)disulfanyl]benzoic acid #8211;4,4 #8242;-bipyridyl N,N #8242;-dioxide (1/2)

In the title 2:1 adduct, C14H10O4S2·0.5C10H8N2O2, which arose from an unexpected oxidation of a precursor, the dihedral angle between the aromatic rings in the disulfide is 82.51 (11)°. In the crystal, the molecules are linked by O—H...O, O—H...N and C...

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Veröffentlicht in:Acta crystallographica. Section E, Structure reports online Structure reports online, 2010-06, Vol.66 (6), p.o1442-o1442
Hauptverfasser: Rodolfo Moreno-Fuquen, Javier Ellena, Carlos A. De Simone, Leandro Ribeiro, Regina Helena De Almeida Santos
Format: Artikel
Sprache:eng
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Zusammenfassung:In the title 2:1 adduct, C14H10O4S2·0.5C10H8N2O2, which arose from an unexpected oxidation of a precursor, the dihedral angle between the aromatic rings in the disulfide is 82.51 (11)°. In the crystal, the molecules are linked by O—H...O, O—H...N and C—H...O interactions, generating sheets.
ISSN:1600-5368
1600-5368
DOI:10.1107/S1600536810018775