P -[ N -(Diphenylphosphorothioyl)isopropylamino]- N -isopropyl- P -phenylthiophosphinic amide

P -[ N -(Diphenylphosphorothioyl)isopropylamino]- N -isopropyl- P -phenylthiophosphinic amide

The title compound, C24H30N2P2S2, was obtained by the reaction of Ph2PN(iPr)P(Ph)N(iPr)H with elemental sulfur in tetrahydrofuran. In the solid state, intramolecular N—H...S hydrogen bonding influences the molecular conformation; a P—N—P—N torsion angle of 2.2...

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Veröffentlicht in:Acta crystallographica. Section E, Structure reports online Structure reports online, 2009-05, Vol.65 (5), p.o1084-o1084
Hauptverfasser: Peulecke, Normen, Aluri, Bhaskar R., Wöhl, Anina, Spannenberg, Anke, Al-Hazmi, Mohammed H.
Format: Artikel
Sprache:eng
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Beschreibung
Zusammenfassung:The title compound, C24H30N2P2S2, was obtained by the reaction of Ph2PN(iPr)P(Ph)N(iPr)H with elemental sulfur in tetrahydrofuran. In the solid state, intramolecular N—H...S hydrogen bonding influences the molecular conformation; a P—N—P—N torsion angle of 2.28 (9)° is observed. The two phenyl rings attached to one P atom form a dihedral angle of 74.02 (4)°.
ISSN:1600-5368
1600-5368
DOI:10.1107/S1600536809014238