N-[2-(4-Bromo-phen-yl)-5-methyl-4-oxo-1,3-thia-zolidin-3-yl]pyridine-3-carboxamide

In the title compound, C(16)H(14)BrN(3)O(2)S, the atoms of the 1,3-thia-zolidine group, except for the N and the C atoms attached to the bromo-benzene ring, are disordered over two sets of sites with occupancies of 0.605 (13) and 0.395 (13). The benzene and pyridine rings make a dihedral angle of 86...

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Veröffentlicht in:Acta crystallographica. Section E, Structure reports online Structure reports online, 2011-04, Vol.67 (Pt 4), p.o914-o915
Hauptverfasser: Akkurt, Mehmet, Celik, Ismail, Demir, Hale, Ozkırımlı, Sumru, Büyükgüngör, Orhan
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Sprache:eng
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Zusammenfassung:In the title compound, C(16)H(14)BrN(3)O(2)S, the atoms of the 1,3-thia-zolidine group, except for the N and the C atoms attached to the bromo-benzene ring, are disordered over two sets of sites with occupancies of 0.605 (13) and 0.395 (13). The benzene and pyridine rings make a dihedral angle of 86.2 (2)°. In the crystal, mol-ecules are linked by inter-molecular N-H⋯N and C-H⋯O hydrogen bonds, forming a three-dimensional network. Furthermore, there is a π-π stacking inter-action [centroid-centroid distance = 3.758 (2) Å] between the pyridine and benzene rings.
ISSN:1600-5368
1600-5368
DOI:10.1107/S1600536811009603