Microwave Synthesis of (4-hydroxy Phenyl) 3-oxo butanoate
The product 3 was previously prepared [1] using C6H6 in the presence of pyridine. A mixture of hydroquinone 1 (0.66 g, 6 mmol), ethyl acetoacetate 2 (0.78 g, 6 mmol) and monmorillonite K10 (0.43 g, 30 % by weight of the total reactants) [2,3] was placed in a pyrex tube which was then introduced into...
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Veröffentlicht in: | MolBank 2008-03, Vol.2008 (1), p.M561 |
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Hauptverfasser: | , , , |
Format: | Artikel |
Sprache: | eng |
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Zusammenfassung: | The product 3 was previously prepared [1] using C6H6 in the presence of pyridine. A mixture of hydroquinone 1 (0.66 g, 6 mmol), ethyl acetoacetate 2 (0.78 g, 6 mmol) and monmorillonite K10 (0.43 g, 30 % by weight of the total reactants) [2,3] was placed in a pyrex tube which was then introduced into a Maxidigest MX 350 Prolabo microwave monomode reactor fitted with a rotational system [4]. |
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ISSN: | 1422-8599 1422-8599 |
DOI: | 10.3390/M561 |