Facile solvothermal synthesis of bimetallic CoMoS2 and NiMoS2 nanospheres

Facile solvothermal synthesis of bimetallic CoMoS2 and NiMoS2 nanospheres

Bimetallic nickel or cobalt molybdenum disulfide (MMoS , M=Ni or Co) nanospheres, with a diameter ranging between 450 nm and 1 μm, have been successfully synthesized using a mild solvothermal method. The obtained nanomaterials have been comprehensively characterized using transmission electron micro...

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Veröffentlicht in:Green processing and synthesis 2015-10, Vol.4 (5), p.379-388
Hauptverfasser: Akram, Hanane, Mateos-Pedrero, Cecilia, Gallegos-Suárez, Esteban, Guerrero-Ruíz, Antonio, Chafik, Tarik, Rodríguez-Ramos, Inmaculada
Format: Artikel
Sprache:eng
Schlagworte:
CoMoS
comos2
MoS
mos2
nanospheres
NiMoS
nimos2
solvothermal synthesis
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Zusammenfassung:Bimetallic nickel or cobalt molybdenum disulfide (MMoS , M=Ni or Co) nanospheres, with a diameter ranging between 450 nm and 1 μm, have been successfully synthesized using a mild solvothermal method. The obtained nanomaterials have been comprehensively characterized using transmission electron microscopy (TEM), high resolution TEM (HRTEM), energy-dispersive X-ray spectroscopy (EDX), X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FT-IR), thermogravimetry analysis (TGA), X-ray photoelectron spectroscopy (XPS) and temperature-programmed reduction (TPR).
ISSN:2191-9542
2191-9550
DOI:10.1515/gps-2015-0017