Ball-milling synthesized Bi2VO5.5 for piezo-photocatalytic assessment
The mechanochemical ball milling followed by heating at 650 °C for 5 h successfully produced the single-phase Bi 2 VO 5.5 powder. Catalytic activity for methylene blue dye degradation was investigated. Raman spectroscopy and X-ray diffraction were used to confirm the phase formation. The sample’s ch...
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Veröffentlicht in: | Scientific reports 2023-05, Vol.13 (1), p.8188-8188, Article 8188 |
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Sprache: | eng |
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Zusammenfassung: | The mechanochemical ball milling followed by heating at 650 °C for 5 h successfully produced the single-phase Bi
2
VO
5.5
powder. Catalytic activity for methylene blue dye degradation was investigated. Raman spectroscopy and X-ray diffraction were used to confirm the phase formation. The sample’s charge carrier transportation behavior was ascertained using time-dependent photocurrent analysis. The piezo-photocatalysis experiment yielded a 63% degradation efficiency for the ball-milled Bi
2
VO
5.5
sample. The pseudo-first-order kinetics of the piezo-photocatalytic dye degradation are discerned, and the significant k value of 0.00529 min
−1
is achieved. The scavenger test declares the h
+
radical is the predominant active species during the piezo-photocatalysis experiment. Vigna radiata seeds were used in a phytotoxicity test to evaluate the germination index. The mechanochemical activation method facilitates reactions by lowering reaction temperature and time. The effect of improved piezo-photocatalytic efficiency on the ball-milled Bi
2
VO
5.5
powder is an unexplored area, and we have attempted to investigate it. Here, ball-milled Bi
2
VO
5.5
powder achieved improved dye degradation performance. |
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ISSN: | 2045-2322 2045-2322 |
DOI: | 10.1038/s41598-023-33658-2 |