Ball-milling synthesized Bi2VO5.5 for piezo-photocatalytic assessment

The mechanochemical ball milling followed by heating at 650 °C for 5 h successfully produced the single-phase Bi 2 VO 5.5 powder. Catalytic activity for methylene blue dye degradation was investigated. Raman spectroscopy and X-ray diffraction were used to confirm the phase formation. The sample’s ch...

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Veröffentlicht in:Scientific reports 2023-05, Vol.13 (1), p.8188-8188, Article 8188
Hauptverfasser: Kumar, Manish, Vaish, Rahul, Kebaili, Imen, Boukhris, Imed, Kwang Benno Park, Hyeong, Hwan Joo, Yun, Hyun Sung, Tae, Kumar, Anuruddh
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Sprache:eng
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Zusammenfassung:The mechanochemical ball milling followed by heating at 650 °C for 5 h successfully produced the single-phase Bi 2 VO 5.5 powder. Catalytic activity for methylene blue dye degradation was investigated. Raman spectroscopy and X-ray diffraction were used to confirm the phase formation. The sample’s charge carrier transportation behavior was ascertained using time-dependent photocurrent analysis. The piezo-photocatalysis experiment yielded a 63% degradation efficiency for the ball-milled Bi 2 VO 5.5 sample. The pseudo-first-order kinetics of the piezo-photocatalytic dye degradation are discerned, and the significant k value of 0.00529 min −1 is achieved. The scavenger test declares the h + radical is the predominant active species during the piezo-photocatalysis experiment. Vigna radiata seeds were used in a phytotoxicity test to evaluate the germination index. The mechanochemical activation method facilitates reactions by lowering reaction temperature and time. The effect of improved piezo-photocatalytic efficiency on the ball-milled Bi 2 VO 5.5 powder is an unexplored area, and we have attempted to investigate it. Here, ball-milled Bi 2 VO 5.5 powder achieved improved dye degradation performance.
ISSN:2045-2322
2045-2322
DOI:10.1038/s41598-023-33658-2