An approximate in-situ method for investigating irradiation damage of grain boundary
•An approximate in-situ method, MCII was proposed to investigate irradiation damage.•MCII uses a conventional ion accelerator and a separated TEM.•MCII can be applied to investigate the irradiation effects of grain boundaries.•The feasibility of MCII was verified in both low- and high-angle boundari...
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Veröffentlicht in: | Nuclear materials and energy 2021-12, Vol.29, p.101056, Article 101056 |
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Hauptverfasser: | , , , , , , , |
Format: | Artikel |
Sprache: | eng |
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Zusammenfassung: | •An approximate in-situ method, MCII was proposed to investigate irradiation damage.•MCII uses a conventional ion accelerator and a separated TEM.•MCII can be applied to investigate the irradiation effects of grain boundaries.•The feasibility of MCII was verified in both low- and high-angle boundaries.
Grain boundary plays an important role in irradiation damage. The presented work proposes an approximate in-situ method, mesh-covered ion irradiation (MCII) for investigating the irradiation damage. The method was applied to a Fe-9 wt.% Al model alloy. During irradiation, transmission electron microscopy (TEM) samples prepared by twin-jet electro-polishing were covered by 400-Cu gilder grids with a pitch of 62 µm, a hole width of 37 µm, and a bar width of 25 µm. After He irradiations, in both the high-angle boundary and the sub-grain boundary, the irradiated and non-irradiated zones can be simultaneously generated. The MCII method provides an approximate in-situ method to investigate irradiation damage of grain boundaries when separately using a conventional ion accelerator and a TEM. |
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ISSN: | 2352-1791 2352-1791 |
DOI: | 10.1016/j.nme.2021.101056 |