An approximate in-situ method for investigating irradiation damage of grain boundary

•An approximate in-situ method, MCII was proposed to investigate irradiation damage.•MCII uses a conventional ion accelerator and a separated TEM.•MCII can be applied to investigate the irradiation effects of grain boundaries.•The feasibility of MCII was verified in both low- and high-angle boundari...

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Veröffentlicht in:Nuclear materials and energy 2021-12, Vol.29, p.101056, Article 101056
Hauptverfasser: Zhang, Lei, Du, Yufeng, Han, Wentuo, Liu, Pingping, Yi, Xiaoou, Yabuuchi, Kiyohiro, Ohnuki, Somei, Wan, Farong
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Sprache:eng
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Zusammenfassung:•An approximate in-situ method, MCII was proposed to investigate irradiation damage.•MCII uses a conventional ion accelerator and a separated TEM.•MCII can be applied to investigate the irradiation effects of grain boundaries.•The feasibility of MCII was verified in both low- and high-angle boundaries. Grain boundary plays an important role in irradiation damage. The presented work proposes an approximate in-situ method, mesh-covered ion irradiation (MCII) for investigating the irradiation damage. The method was applied to a Fe-9 wt.% Al model alloy. During irradiation, transmission electron microscopy (TEM) samples prepared by twin-jet electro-polishing were covered by 400-Cu gilder grids with a pitch of 62 µm, a hole width of 37 µm, and a bar width of 25 µm. After He irradiations, in both the high-angle boundary and the sub-grain boundary, the irradiated and non-irradiated zones can be simultaneously generated. The MCII method provides an approximate in-situ method to investigate irradiation damage of grain boundaries when separately using a conventional ion accelerator and a TEM.
ISSN:2352-1791
2352-1791
DOI:10.1016/j.nme.2021.101056