Determination of selenium in infant foods using electrothermal atomic absorption spectrometry with direct slurry sample introduction

Slurry sampling electrothermal atomic absorption (SS ETAAS) was applied to the development of a sensitive and precise method for selenium determination in infant foods without sample pretreatment. Suspensions prepared in a medium containing 0.1% Triton X-100, 0.5 or 5% v/v concentrated HNO3 were dir...

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Veröffentlicht in:Open Chemistry 2004-06, Vol.2 (2), p.334-346
Hauptverfasser: Baralkiewicz, Danuta, El-Sayed, Usama, Filipiak, Marian, Gramowska, Hanka, Mleczek, Miroslaw
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Sprache:eng
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Zusammenfassung:Slurry sampling electrothermal atomic absorption (SS ETAAS) was applied to the development of a sensitive and precise method for selenium determination in infant foods without sample pretreatment. Suspensions prepared in a medium containing 0.1% Triton X-100, 0.5 or 5% v/v concentrated HNO3 were directly introduced into the furnace. The accuracy of the procedure was confirmed by analysis of a standard reference material and comparison with hydride generation atomic absorption spectrometric (HGAAS) procedure. The characteristic mass is 44 pg and detection limit 0.43 μg·l−1.
ISSN:2391-5420
2391-5420
DOI:10.2478/BF02475577