The synthesis and the structure elucidation of N,O-diacetyl derivative of cyclic 3-hydroxymelatonin

The synthesis and the structure elucidation of N,O-diacetyl derivative of cyclic 3-hydroxymelatonin

Melatonin was subjected to an oxidation to give 3-hydroxymelatonin. All spectroscopic data for this compound were collected. Ab initio calculations for both possible configurations were performed. X-ray data on N,O-diacetyl derivative of 3-hydroxymelatonin allowed the unambigous structure determinat...

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Veröffentlicht in:Open Chemistry 2004-09, Vol.2 (3), p.425-433
Hauptverfasser: Siwicka, Aleksandra, Reiter, Russel, Tian, Dun, Wojtasiewicz, Krystyna, Leniewski, Andrezej, Maurin, Jan, Błachut, Dariusz, Czarnocki, Zbigniew
Format: Artikel
Sprache:eng
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alkaloids
anti-cancer activity
antioxidants
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Zusammenfassung:Melatonin was subjected to an oxidation to give 3-hydroxymelatonin. All spectroscopic data for this compound were collected. Ab initio calculations for both possible configurations were performed. X-ray data on N,O-diacetyl derivative of 3-hydroxymelatonin allowed the unambigous structure determination.
ISSN:2391-5420
2391-5420
DOI:10.2478/BF02476198